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USGS Spectral Library Version 7 Sample Description

Kokaly, R.F., Clark, R.N., Swayze, G.A., Livo, K.E., Hoefen, T.M., Pearson, N.C., Wise, R.A., Benzel, W.M., Lowers, H.A., Driscoll, R.L., and Klein, A.J., 2017, USGS Spectral Library Version 7: U.S. Geological Survey Data Series 1035, 61 p., https://doi.org/10.3133/ds1035
For more information on the library, see: local link web link

TITLE: Ulexite HS441 DESCRIPT

DOCUMENTATION_FORMAT: MINERAL

SAMPLE_ID: HS441.1B, HS441.2B, HS441.3B, HS441.4B

MINERAL_TYPE: Borate

MINERAL: Ulexite

FORMULA: NaCaB5O9*8H2O

FORMULA_HTML: NaCaB5O9•8H2O

COLLECTION_LOCALITY: California

ORIGINAL_DONOR: Hunt and Salisbury Collection

CURRENT_SAMPLE_LOCATION: USGS Denver Spectroscopy Laboratory

ULTIMATE_SAMPLE_LOCATION: USGS Denver Spectroscopy Laboratory

SAMPLE_DESCRIPTION:

Hydrous borate.

Grain size fractions are indicated by the extension after the sample number:
.1B = <5 µm
.2B = <74 µm
.3B = 74-250 µm
.4B = 250-1200 µm

IMAGE_OF_SAMPLE:
Photo of sample

END_SAMPLE_DESCRIPTION.

XRD_ANALYSIS:

40 kV - 30 mA, 6.5-9.5 keV [smear mount of ground sample is ulexite.out, bulk mount or random mount of unground sample is ulexite2.out]
References: JCPDS #12-419 (from Clark and Christ, 1959; Ghose and others, 1978)
Found: Ulexite

Comments: There are so many peaks that reflections of a second phase, if present could be obscured by overlap. Pattern ulexite2.out is extraordinary and was indexed successfully to about 35 degrees 2 theta using powder intensities calculated from the structure of Ghose and others (1978). Reflections are very sharp, indicating a high degree of crystallinity and compositional heterogeneity.

J.S. Huebner and J. Pickrell, unpublished data, written communication, USGS, Reston, VA (1993)

END_XRD_ANALYSIS.

COMPOSITIONAL_ANALYSIS_TYPE: None # XRF, EPMA, ICP(Trace), WChem

COMPOSITION_TRACE: None

COMPOSITION_DISCUSSION:

None

END_COMPOSITION_DISCUSSION.

MICROSCOPIC_EXAMINATION:

END_MICROSCOPIC_EXAMINATION.

SPECTROSCOPIC_DISCUSSION:

END_SPECTROSCOPIC_DISCUSSION.

SPECTRAL_PURITY: 1a2_3_4_ # HS441.1B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns
SPECTRAL_PURITY: 1a2_3_4_ # HS441.2B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns
SPECTRAL_PURITY: 1a2a3a4_ # HS441.3B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns
SPECTRAL_PURITY: 1a2_3_4_ # HS441.4B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns