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USGS Spectral Library Version 7 Sample Description

Kokaly, R.F., Clark, R.N., Swayze, G.A., Livo, K.E., Hoefen, T.M., Pearson, N.C., Wise, R.A., Benzel, W.M., Lowers, H.A., Driscoll, R.L., and Klein, A.J., 2017, USGS Spectral Library Version 7: U.S. Geological Survey Data Series 1035, 61 p., https://doi.org/10.3133/ds1035
For more information on the library, see: local link web link

TITLE: Quartz HS32 DESCRIPT

DOCUMENTATION_FORMAT: MINERAL

SAMPLE_ID: HS32.1B, HS32.2B, HS32.3B, HS32.4B

MINERAL_TYPE: Tectosilicate

MINERAL: Quartz

FORMULA: SiO2

FORMULA_HTML: SiO2

COLLECTION_LOCALITY: Rock Springs, Arkansas

ORIGINAL_DONOR: Hunt and Salisbury Collection

CURRENT_SAMPLE_LOCATION: USGS Denver Spectroscopy Laboratory

ULTIMATE_SAMPLE_LOCATION: USGS Denver Spectroscopy Laboratory

SAMPLE_DESCRIPTION:

This particular sample is a very pure variety of clear crystal quartz, and careful grinding has produced a sample with very high reflectivity and almost devoid of spectral features. There are only two very weak features at 2.3 and 2.5µm in the finest grain sizes. Because there are no bands at 1.4µm or 1.9µm, these features cannot be attributed to water or hydroxyl groups in the quartz. The cross-overs of the two very fine grain sizes with the others is not significant.

Hunt, G.R., J.W. Salisbury, 1970, Visible and near-infrared spectra of minerals and rocks: I. Silicate minerals. Modern Geology, v. 1, p. 283-300.

Results of petrographic examination: Crystal clear quartz.

Salisbury, J. W., Walter, L. W., and Vergo, N., 1987, Mid-Infrared (2.1-25µm) Spectra of Minerals: First Edition, U.S. Geological Survey Open File Report 87-263.

Grain size fractions are indicated by the extension after the sample number:
.1B = <5 µm
.2B = <74 µm
.3B = 74-250 µm
.4B = 250-1200 µm

IMAGE_OF_SAMPLE:
Photo of sample

END_SAMPLE_DESCRIPTION.

XRD_ANALYSIS:

Pure. (Norma Vergo)

Pure quartz.

Salisbury, J. W., Walter, L. W., and Vergo, N., 1987, Mid-Infrared (2.1-25µm) Spectra of Minerals: First Edition, U.S. Geological Survey Open File Report 87-263.

END_XRD_ANALYSIS.

COMPOSITIONAL_ANALYSIS_TYPE: None # XRF, EPMA, ICP(Trace), WChem

COMPOSITION_TRACE:

COMPOSITION_DISCUSSION:

Results of XRF or other compositional analysis: Essentially pure SiO2 within the limit of microprobe error.

Salisbury, J. W., Walter, L. W., and Vergo, N., 1987, Mid-Infrared (2.1-25µm) Spectra of Minerals: First Edition, U.S. Geological Survey Open File Report 87-263.

END_COMPOSITION_DISCUSSION.

MICROSCOPIC_EXAMINATION:

Colorless transparent. No contamination visually apparent.

END_MICROSCOPIC_EXAMINATION.

SPECTROSCOPIC_DISCUSSION:

Possible residual artifact from incomplete removal of spectralon feature at 2.1 microns. This is not present in the Beckman spectrum of the 4B sample. Alternatively, the 1.9 and 2.2 micron absorptions could be due to Si-OH (silanol) absorptions that may be humidity dependent.

See: Swayze, G.A., Clark, R.N., Goetz, F.H., Livo, K.E., Breit, G.N., Kruse, F.A., Sutley, S.J., Snee, L.W., Lowers, H.A., Post, J.L., Stoffregen, R.E. and Ashley, R.P., 2014, Mapping advanced argillic alteration at Cuprite, Nevada using imaging spectroscopy: Economic Geology, v. 109, no. 5, p. 1179-1221.

END_SPECTROSCOPIC_DISCUSSION.

SPECTRAL_PURITY: 1c2_3_4_ # HS32.1B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns
SPECTRAL_PURITY: 1c2_3_4_ # HS32.2B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns
SPECTRAL_PURITY: 1c2_3_4_ # HS32.3B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns
SPECTRAL_PURITY: 1a2_3_4_ # HS32.4B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns