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USGS Spectral Library Version 7 Sample Description

Kokaly, R.F., Clark, R.N., Swayze, G.A., Livo, K.E., Hoefen, T.M., Pearson, N.C., Wise, R.A., Benzel, W.M., Lowers, H.A., Driscoll, R.L., and Klein, A.J., 2017, USGS Spectral Library Version 7: U.S. Geological Survey Data Series 1035, 61 p., https://doi.org/10.3133/ds1035
For more information on the library, see: local link web link

TITLE: Actinolite HS22 DESCRIPT

DOCUMENTATION_FORMAT: MINERAL

SAMPLE_ID: HS22.1B, HS22.2B, HS22.3B, HS22.4B

MINERAL_TYPE: Inosilicate

MINERAL: Actinolite (Amphibole group)

FORMULA: Ca2(Mg,Fe+2)5Si8O22(OH)2

FORMULA_HTML: Ca2(Mg,Fe+2)5Si8O22(OH)2

COLLECTION_LOCALITY: Chester, VT.

ORIGINAL_DONOR: Hunt and Salisbury Collection

CURRENT_SAMPLE_LOCATION: USGS Denver Spectroscopy Laboratory

ULTIMATE_SAMPLE_LOCATION: USGS Denver Spectroscopy Laboratory

SAMPLE_DESCRIPTION:

Forms a series with Tremolite and Ferro-actinolite.

Original spectrum published in:

Hunt, G.R., J.W. Salisbury, 1970, Visible and near-infrared spectra of minerals and rocks: I. Silicate minerals. Modern Geology, vol. 1, pp283-300, with the note: "The flattening of the spectral curve of the finest size range near 2 µm, which produces a cross-over of the spectra, is apparently due to a very slight contamination of the sample by opaque inclusions of pyrite (?)."

A spectrum of this sample is also published in: Clark, R.N., T.V.V. King, M. Klejwa, G. Swayze, and N. Vergo, 1990, High spectral resolution reflectance spectroscopy of minerals: J. Geophys Res., v. 95, 12653-12680, who noted that the sample is spectrally pure.

Grain size fractions are indicated by the extension after the sample number:
.1B = <5 µm
.2B = <74 µm
.3B = 74-250 µm
.4B = 250-1200 µm

IMAGE_OF_SAMPLE:
Photo of sample

END_SAMPLE_DESCRIPTION.

XRD_ANALYSIS:

40 kV - 30 mA, 7.3-9.5 keV
File: acHS22.out, *_mdi (smear mount on quartz plate)
References: Huebner's reference patterns
Found: Clinoamphibole, chlorite, trace possible talc

Comment: Excellent amphibole pattern closely matches that of a natural tremolite-actinolite. Insufficient number of chlorite reflections to determine polytype. Weak reflection at 9.2 Angstroms could be the strong basal reflection of talc, which commonly occurs with tremolite-actinolite.

J.S. Huebner, J. Pickrell, T. Schaefer, written communication 1994.

END_XRD_ANALYSIS.

COMPOSITIONAL_ANALYSIS_TYPE: EPMA # XRF, EPMA, ICP(Trace), WChem


COMPOSITION
KEYWORD
Oxide
ASCII
Amount Weight
Percent, %
Oxide
html
COMPOSITION: SiO2 54.53 wt% SiO2
COMPOSITION: TiO2 0.04 wt% TiO2
COMPOSITION: Al2O3 1.64 wt% Al2O3
COMPOSITION: Cr2O3 0.27 wt% Cr2O3
COMPOSITION: FeO 5.46 wt% FeO
COMPOSITION: MnO 0.21 wt% MnO
COMPOSITION: MgO 21.69 wt% MgO
COMPOSITION: CaO 12.01 wt% CaO
COMPOSITION: Na2O 0.41 wt% Na2O
COMPOSITION: K2O 0.03 wt% K2O
COMPOSITION: Total 96.28 wt%
COMPOSITION: O=Cl,F,S wt% #correction for Cl, F, S
COMPOSITION: New Total wt%

COMPOSITION_TRACE: None

COMPOSITION_DISCUSSION:

EM analysis by Gregg A. Swayze at USGS Branch of Geophysics, Denver, indicates stoichiometric actinolite.

END_COMPOSITION_DISCUSSION.

MICROSCOPIC_EXAMINATION:

Optical examination give the following mineral mode:

91.5 vol% actinolite
8.0 vol% wh. mica or calcite
0.5 vol% opaque inclusions

avg. grain size = 74-250µm

Mostly pure, highly fractured green actinolite grains (occasionally some with opaque inclusions). Platy translucent mica? grains intermixed with actinolite. Continuous grain size distribution with little coating of larger grains by smaller grains. G. Swayze

END_MICROSCOPIC_EXAMINATION.

SPECTROSCOPIC_DISCUSSION:

END_SPECTROSCOPIC_DISCUSSION.

SPECTRAL_PURITY: 1b2_3_4_ # HS22.1B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns
SPECTRAL_PURITY: 1b2_3_4_ # HS22.2B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns
SPECTRAL_PURITY: 1b2b3b4b # HS22.3B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns
SPECTRAL_PURITY: 1b2_3_4_ # HS22.4B # 1= 0.2-3, 2= 1.5-6, 3= 6-25, 4= 20-150 microns